By Dan P. Manka
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Extra info for Automated Stream Analysis for Process Control. Volume 1
A c c o r d i n g to chemical reactor engineering theory as presented by T a y l o r ( 1 9 5 3 ) , l a m i n a r flow in open bore tubular reactors results in plug flow w h e r e b y , a m o n g other t h i n g s , the linear velocity of the flowing stream is zero at the l i q u i d - w a l l interface. If this w e r e universally true, the excellent s h o r t - t e r m baseline resolution exhibited in F I A w o u l d be impossible. A l t h o u g h the exact m e c h a n i s m of action of m a s s transport under F I A condi tions is not entirely u n d e r s t o o d , V a n d e r s l i c e et al.
2. 48 to Detector (b) Fig. 8. (a) Automated determination of cationic surfactants using segmented flow analysis, (b) Automated determination of cationic surfactants using flow-injection analysis. Finally, an e x a m p l e of the excellent quantitative aspect of solvent extraction by F I A is p r e s e n t e d in F i g . 9. Both c h r o m a t o g r a m s w e r e run on p o l y n u c l e a r aromatic h y d r o c a r b o n s extracted from oil (Shelly, 1982). A s is evident, the F I A extraction d e m o n s t r a t e s an excellent correlation with the m a n u a l extraction.
1. Typical recorder output of transient peaks associated with FIA limited and medium dispersion conditions. 5 6 8 10 From P r o c e s s S t r e a m Fig. 2. Generalized schematic of Lachat QuikChem™ process monitor: (1) sample suction pump, (2) in-line filter, (3) standard solution, (4) rinsing solution, (5) 3-way solenoid valve, (6) sample injection valve, (7) primary reagent or diluent, (8) reaction manifold, (9) additional reagents, (10) detector, (11) recorder, (12) microprocessor, (13) analog or digital data transmission line, (14) h i - l o alarm, (15) automatic drift correction, and (16) automatic recalibration.
Automated Stream Analysis for Process Control. Volume 1 by Dan P. Manka